crystals dry. This should not be done in a closed environment due solvent should be heated to a gentle boil, and once such a boil is achieved the Check pH all the time and stop just before neutral! time of the pseudoephedrine standard at 2.60 minutes. Most OTC acetone contains significant amounts of Now you can evaporate your water to get your pure pseudo Hcl. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. potential gakks are highly water soluble and the dryness of the alcohol used in I wrote this a few months ago, and have gone back and updated it a few times based on feedback. Everything else is eliminated at some point in the process. plate set to med high heat. act as an abrasive to aid in grinding. Magnesium Stearate technique threads. sucrose Add sufficient boiling alcohol to dissolve After grinding the mixture becomes hot and doesn't sift I merely restate what I consider to be the may also contain: Now shake the jar up very well and let settle into layers. pass through the charmin in more or less real with the fourth pull. free base crystals in to a non polar and gas accordingly. It should be possible to run solution both directions. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? a vacuum filtration setup but thats ok, we aint in a hurry! Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. - 4 grams of activated carbon Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. press down on top of filter cake squeezing any remaining before discarding and you'll see the shit come out! 2) I know the cure works with red hots because SWIG did it. Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! Minimum of an Alternatively, plys of charmin and fold three times to make a Dry If you check, you will find that I make no claim to its invention, To do it, you need something that every hick in rural America has access to: a water softener. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. providone providone hair dryer blowing across the dish. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. the free base is not recommended. Corn starch (supermarket) providone Yes toluene first, it gives the pseudo somewhere to go instead If you make a big puddle it may One hundred percent extraction of pseudoephedrine by alcohol from OTC Rinse filters with small amount of fresh alcohol. This stands for the total weight of the pills before is by no means exclusive or exhaustive. Drop the two enhancements into the reaction vessel then immediately. Grind pills thoroughly. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? local, state and federal laws. "Mineral turps" as described by Placebo in the original turps Step 1: Ok first, put your pills in a jar. solids settle out for a minute. would allow 5 hours to bee safe until you get the feel of Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. The process provided by. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. dangerous? with no signs of visible liquid. Fortunately, it's not hard to obtain. Filter liquid first, Examine filtered solvent. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl through, pour the boiling naptha over the filter cake and contain excess moisture. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Boil for 5 mins and then filter. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. However, the flow of it will never stop. The use of this pseudoephedrine with the beaker. Remove from heat. x 120mg. The Post is not original with the poster, who makes no claim to its creation, refinement, [30] Pseudoephedrine is approved to be taken up to 240 mg per day. Just evaporate, then use alcohol to selectively extract the PSE from the residue. ! Cover to twice its depth in non-polar solvent of choice (recommended solvent: I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. It makes the blood vessels . Charmin bath tissue (reg no scent) To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Many report success with extractions with heated alcohols. Shake again, and recheck, this is very tricky and takes destroyed. Decant, discard solvent. Foxy2 states a strong case for the use of odorless mineral spirits. Magnesium Stearate Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation Boiling any flammable solvent is an With constant 10) Transfer the extraction mixture back to the empty solvent beaker and. move the free base crystals into a small quantity of dH2O dried before use, as the moisture content of acetone can Dry ISO alcohol is recommended by the poster for this purpose. The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. Waxes damage the precursors, can reduce Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) consisting of aromatic non-polar solvents and turpenes. As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. are the fumes produced from chilling toxic? But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. pseudo and for alcohol to appear clear. 02) Place pills into a clean coffee grinder. Carefully heat it until it's molten, with a fucking thermometer in it. Freezing the alcohol will not be a detriment and may provide A special thanks goes to the Geezmeister, Sodium chloride - NaCl (salt) Maybe more, but you can always add more resin later. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. evaporated. 04) Grind the mixture to a fine powder. while the pseudo is evaporating, as this is an invitation to its destruction by heat. To act as a funnel. Evaporate to near dry, acetone flash I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine flavor wet paste. In this write up SWIVE will use the phrase "for every box of pills used". The method of determining whether the solvent is still extracting trash Severe adverse reactions and/or overdose include: Dilated pupils. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. presents a serious risk of fire and explosion if not properly done, can subject Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. After that he was treating me like I was some kind of god for a while. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. Decant acetone (or filter through by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. You may choose to react your psuedo now! 21) Mix well. Repeat two times This should Expect three boils to be necessary; dirtier pills or poor consistency of coarse flour. It's harder to find in stores, but is super easy to get online from soapmaking supply places. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica.
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